一、概 述
孔隙度是岩石的重要性质之一,它定义为孔隙体积与岩石几何体积的比值,通常用百分数表示。这种油田水烃类物质占据的孔隙空间的大小,无论对合理评价油藏,还是对油藏进行工程施工都是必不可少的参数。
我们参考了大量的资料设计的气体孔隙度仪,具有结构简单、操作方便、测定速度快、性能稳定等特点,是岩心分析实验室必不可少的装置。
二、工作原理
气体孔隙度仪是测量体积的一种仪器,用它可以测定岩样的骨架体积和孔隙度体积,利用气体膨胀原理,即玻义尔(BoyLE)定律,已知体积的气体在确定的压力下向未知体积等温膨胀,膨胀后可测定终的平衡压力。平衡压力的大小取决于未知体积的大小,而未知体积的大小由玻义尔定律求得。
该仪器可用两种气体作为驱替介质,氮气和氦气。对于一般的砂岩可用氮气,对于较为致密的灰岩和孔隙较小的岩样可用氦气测定。用氦气的理由是:①微小的氦气(分子分子半径r=0.9A)作为介质能够进入与油藏岩石伴生的毛细管;②分子量低的氦气(M=4)对岩石具有较高的渗透能力;③岩石表面对氦气吸咐性较差。
根据玻义尔定律:气体的已知体积Vk与所测压力Pk下等温膨胀到未知室体积V中,膨胀后测量终平衡压力P这个平衡压力取决于未知体积量,未知体积可以用玻义尔定律求得。
三、仪器结构及各部件说明
本仪器是根据玻义尔定律设计的,所以等温很重要,故要求安装在非通气区,没有空气直接流通的室内实验台上,只要温度稳定在2%范围内,即可测得稳定的结果。
仪器有下列部件:
1.气源阀:供给孔隙计调节器低于1MPa氦(氮)气,当供气阀关闭时,调节器通过常泄,使压力保持恒定。
2.调节器:将1MPa的压力准确地调节到0.7MPa以下。
3.供气阀:连接0.7MPa以下压力的气体到标准室和压力计,它是标准室体积的上游极限。
4.标准室:已知体积室。
5.样品阀:能使标准室内0.7MPa压力的气体连接到未知室体积上去,它是标准室体积的下游极限。
6.放空阀:使末知体积中的初始压力为0MPa,同时又可以使平衡后的气体放入大气。
7.压力计:测量体系中气体压力,用来指示标准室的压力准确达到0.7MPa以下,并指示体系平衡的压力。
I. Overview
Porosity is one of the important properties of rock, which is defined as the ratio of pore volume to geometric volume of rock, usually expressed as percentage. The size of pore space occupied by hydrocarbon substances in oilfield water is an essential parameter for reasonable evaluation of oil reservoirs and engineering construction of oil reservoirs.
The gas porosity instrument designed by us with reference to a large number of data has the characteristics of simple structure, convenient operation, fast determination speed and stable performance, and is an essential device in the core analysis laboratory.
Second, the working principle
Gas porosimeter is an instrument for measuring volume, which can be used to measure the skeleton volume and porosity volume of rock samples. By using the principle of gas expansion, that is BoyLE's law, the gas with known volume expands isothermally to the unknown volume at a certain pressure, and the final equilibrium pressure can be determined after expansion. The equilibrium pressure depends on the unknown volume, which is obtained by Boyle's law.
The instrument can use two gases as displacement media, nitrogen and helium. Nitrogen can be used for general sandstone, and helium can be used for dense limestone and small pore rock samples. The reasons for using helium are as follows: ① tiny helium (molecular radius r=0.9A) can enter the capillary associated with reservoir rocks as a medium; ② Helium with low molecular weight (M=4) has high permeability to rocks; ③ The adsorption of helium on the rock surface is poor.
According to Boyle's law, the known volume Vk and the measured pressure Pk of gas expand isothermally into the unknown chamber volume V, and the final equilibrium pressure P is measured after expansion. This equilibrium pressure depends on the unknown volume, and the unknown volume can be obtained by Boyle's law.
III. Instrument Structure and Description of Components
This instrument is designed according to Boyle's law, so isothermal is very important. Therefore, it is required to be installed in an indoor experimental platform in a non-ventilated area without direct air circulation, and stable results can be obtained as long as the temperature is stable within 2%.
The instrument has the following components:
1. Air source valve: helium (nitrogen) gas below 1MPa is supplied to the pore meter regulator. When the air supply valve is closed, the regulator keeps the pressure constant through normal venting.
2. Regulator: Adjust the pressure of 1MPa to below 0.7MPa accurately.
3. Air supply valve: connect the gas with the pressure below 0.7MPa to the standard chamber and pressure gauge, which is the upstream limit of the standard chamber volume.
4. Standard room: a room with known volume.
5. Sample valve: It can connect the gas with pressure of 0.7MPa in the standard room to the unknown room volume, which is the downstream limit of the standard room volume.
6. Vent valve: the initial pressure in the unknown volume is 0MPa, and at the same time, the balanced gas can be released into the atmosphere.
7. Pressure gauge: it measures the gas pressure in the system, and is used to indicate that the pressure in the standard room is below 0.7MPa accurately, and to indicate the equilibrium pressure of the system.
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