SFEC120-50-05超临界二氧化碳萃取装置

    超临界萃取设备升级产品，设备部件工作更稳定，工艺结构合理优化，满足功能需求的前提下，更紧凑美观。
    该装置主要由：萃取釜、分离釜、CO2高压泵、夹带剂泵、制冷系统、CO2贮罐、换热系统、净化系统、流量计、温度控制系统、压力自控系统、安全保护装置、清洗系统等组成。附属设备和系统都能满足超临界萃取主系统的需求和流程图要求。
一、萃取釜：
    配有水夹套循环加热系统，温度可调，配固、液料用料筒
    材质     1Cr18Ni9Ti
    容积     5L
    工作压力  50MPa
二、分离釜：
    配有水夹套循环加热系统，温度可调
    材质     1Cr18Ni9Ti
    容积     2L×2
    工作压力  30MPa
三、CO2高压泵：
    流量（三柱塞）  排量50L/h    变频可调
    工作压力     50MPa    泵头带冷却系统
四、夹带剂泵：
    流量（双柱塞）  1/4～4L/h    机械调节
    工作压力    50MPa
五、制冷系统：
    制冷量    4470Kcal/h   风冷
    温度控制范围    -5℃～+15℃   满足工艺要求
六、换热系统：
    材质      1Cr18Ni9Ti
    规格        Φ6×1
    工作压力   50MPa
    配水夹套循环加热系统，温度可调
七、净化系统：
    材质      1Cr18Ni9Ti
    工作压力   50MPa
八、CO2贮罐：
    材质        1Cr18Ni9Ti
    容积        4L
    工作压力   16MPa
九、流量计：
    金属管质量流量计，量程为6.3~63L/h，带二次仪表
十、温度控制系统：
    控制范围      室温~85℃可调（水浴）
    动态控温精度   ±1℃    数显双屏
十一、安全保护装置：
    高压泵出口配电接点压力表、设定工作压力、超压自动停泵保护。
    萃取釜、分离釜、根据工作压力，分别配安全阀，超压自动泄压。
十二、管路：
    阀门、管件    DW6
    接触流体的容器、阀门、管件、管线均采用1Cr18Ni9Ti不锈钢制作。阀门用阀杆经特殊热处理，坚久耐用。
十三、装置特点：
    萃到釜压环快速打开，O型圈为进口，使用周期4个月以上。
    CO2循环使用。
十四、其它：
    电源：   三相五线制     380V/50HZ     11kW
    CO2：   食品级≥99.5%，单瓶净重≥22Kg  用户自备
    安装尺寸：2700×1200×1750m/m，外加操作空间。

I. Overview:

Supercritical extraction means that at a certain pressure and appropriate temperature, in the extraction cylinder, the solvent fully contacts with the extracted substance, and the solute diffuses into the solvent, and then the working conditions are changed in the separator to precipitate the dissolved substance, so as to achieve the purpose of separation.

Supercritical extraction has the following characteristics:

The extraction temperature is low, and the product will not be decomposed.

Selective extraction can be achieved by controlling temperature and pressure.

There is no solvent residue in the product.

The solvent can be recycled.

No environmental pollution.

Supercritical fluid extraction technology uses CO2 as solvent, which has the following advantages:

The supercritical state of CO2 is easy to realize.

No toxic pollution to food and medicine.

It has the function of preventing bacterial activity.

It is not easy to burn and has good chemical stability.

Low price and good economy.

Second, the device composition process:

The device mainly consists of a refrigeration system, a CO2 storage tank, a mixer, a filter, an extraction kettle, a separation kettle, a CO2 injection pump, a carrier pump, a pressure control system, a flowmeter, a safety protection device, an electric control cabinet, a cabinet frame, a panel and the like.

III. Technical indicators of main components:

3-1. Extraction kettle:

The charging barrel for solid and liquid materials is equipped with a water jacket circulating heating system with adjustable temperature.

Material stainless steel 316

Volume 5L

Working pressure ≤50MPa

3-2, separation kettle:

The main container for material separation, in this process, the separation effect is better by changing the pressure and temperature, and it is equipped with a water jacket circulating heating system with adjustable temperature.

Material stainless steel 316

Two sets with a volume of 2×2L

Working pressure ≤30MPa

3-3, CO2 high-pressure pump:

The CO2 liquid output is pressurized, and the pump head is made of wear-resistant special material and equipped with a cooling circulation system of the pump head, so as to prevent the friction of the pump head from heating up, prolong the service life of the pump, prevent cavitation and affect the stable supply of fluid.

The flow rate is 50L/h and the frequency conversion is adjustable.

Working pressure ≤50MPa

3-4, entrainer pump:

1/4-4L/h mechanical adjustment of flow rate

Working pressure ≤50MPa

3-5, refrigeration system:

The refrigerating capacity is 4700Kcal/h, and it is air cooled.

The temperature control range is 5℃ ~ 7℃

3-6, heat exchange system:

Change the temperature in the system through heat exchange.

Material stainless steel 316

Specification φ 6× 1 coil

Working pressure ≤50MPa

Water distribution jacket circulating heating system with adjustable temperature.

3-7, purification system:

Material stainless steel 316

Working pressure ≤50MPa

3-8, CO2 storage tank:

Material stainless steel 316

Volume 4L

Working pressure 16MPa

3-9, flowmeter:

Metal tube float flowmeter digital display remote transmission 6.3 ~ 63l/h shows instantaneous and cumulative flow respectively.

3-10, temperature control system:

The control range is adjustable from room temperature to 85℃ (water bath)

Dynamic temperature control accuracy 1℃ Double-screen digital display, programmed temperature control.

3-11, cleaning system:

The equipment is designed with a cleaning loop, which can clean the separator first and then clean the whole.

3-12, safety protection device:

Safety system is the most important part of equipment, which is divided into hard safety system and soft safety system.

Hard safety system: a safety control system that can be realized even when the equipment is in the state of no electricity, including safety valves and one-way valves. The main components such as extraction kettle and separation kettle are equipped with their own independent safety valves (the protection pressure is independently calibrated according to the pressure range of the components), and the overpressure is automatically released. After the pressure is normal, it will automatically recover to protect the safety of the components at all times.

Soft safety system: integrated circuit safety control, electric contact pressure instruments, pressure and water level alarm safety control, etc. Once triggered, the soft safety system can not work normally until the problem is solved, and it is ineffective to forcibly start the power device. After the problem is solved, it will return to normal as a necessary supplement to the hard safety system.

Power safety device: the range of system pressure can be set. If the pressure triggers the upper limit, the power output will be stopped to ensure that the system pressure will not rise again. If the pressure is lower than the lower limit, the power output will be started, which can be set as dynamic protection to adjust the safety measures of the equipment, so as to ensure the safety of the equipment.

3-13, pipeline:

The pipeline adopts valve pipe fittings with specifications of DW6/50MPa series and made of stainless steel 316. The valve stem is durable after special heat treatment, and the valve layout fully considers the maintenance and process control of all parts of the equipment.

3-14, electrical system:

Brand electrical components are used for control, and the power cord adopts the three-phase five-wire system of international common standards.

3-15, box bracket:

According to the requirements of modern laboratory, the shape design of the equipment is beautiful and generous. The operation panel is made of stainless steel laser, which is clear at a glance, well arranged and harmonious with modern laboratories.

南通立凯机电工程有限公司专业设计、制造、销售超临界流体设备和石油科研仪器。产品主要包括：
    超临界二氧化碳萃取设备、超临界气凝胶干燥设备、超临界细微粒子制备装置、超临界清洗发泡装置、超临界抗溶剂结晶装置、高温高压磁搅拌反应装置、超临界相平衡仪等。
    岩心自动剖切机、岩心钻取机、岩心钻切机、液氮冷冻钻取机、液氮冷冻切割机、疏松岩心装备装置、岩心端面切磨机、岩心端面切割机、台式切片机、切样机、岩矿切片机、磨片机、单、双盘金相岩相抛光机、颚式破碎机、自动研磨机、岩心快速洗油仪、填砂压实装置、人造岩心制作装置、含粘土人造岩心制作装置、岩心﹙油、水﹚抽空加压饱和实验装置、渗透率自动测定仪、气体渗透率测定仪、全直径岩心渗透率测定仪、克氏渗透率测定仪、氦孔隙度自动测定仪、气体孔隙度测定仪、全直径孔隙度测定仪、气体孔渗联测仪、致密岩心孔渗测定仪、全直径孔渗联测仪、高温覆压孔渗测定仪、岩心饱和度干馏仪、煤岩心测量系统、岩心饱和度干馏仪、全直径岩心饱和度测定仪﹙蒸馏法﹚、碳酸盐含量测定仪﹙表压式﹚、碳酸盐含量测定仪﹙数显式﹚、岩石比面测定仪、岩心流动试验仪、低渗敏感性评价仪、长岩心梯度流动试验仪、特低渗岩心启动压力梯度测量系统、岩心声波综合测试仪、岩心声电渗参数测定仪、岩心电阻率参数测定仪、多功能岩心驱替装置、润湿性测定仪、高压半渗透隔板仪、油、水相对渗透率测定仪、气液相对渗透率仪、高温高压相对渗透率自动测定仪、岩心孔隙铸体仪、岩心力学性能测试系统、长岩心物理模型、多功能综合驱油装置、多维多功能化学驱物理模拟系统、全自动长岩心双管试验装置、聚合物续凝实验装置、天然气水合物的形成及开采、蒸汽驱油试验装置、超临界CO2驱油实验装置、泡沫驱多功能物理模拟实验装置、微观驱物理模拟装置、多层长岩心驱替装置、油藏条件下多功能驱替系统、一维火烧油层实验装置、三维火烧油层实验装置、采油化学剂评价实验装置、天然气水合物抑制评价实验装置、微生物驱油试验装置、振动采油室内模拟试验装置、凝胶转变压力测定仪、全自动过滤因子测定装置、混相仪、动态结垢评价仪、微型蒸汽发生器、油水自动计量装置、油气水自动计量装置、油气水三相自动计量装置、岩心酸化流动试验仪、压裂酸化工作液动滤失仪、堵水调剖流动性能评价仪、支撑剂裂缝导流测试系统、酸蚀裂缝导流仪、酸岩反应旋转岩盘仪、智能高温高压页膨胀仪、高温高压失水仪、动态高温高压养护釜、井壁稳定性模拟实验装置、钻井液高温高压密度特性实验装置、高温高压动态堵漏模拟装置、地层流体高压物性分析仪、深井取样器、原油快速脱水器、原油动态结蜡仪、原油含蜡测定仪、铜板腐蚀试验仪、挂片动态腐蚀仪、活塞式高压配样器、活塞式储样筒、储样筒、岩心夹持器、多测压点岩心夹持器、电阻率岩心夹持器、声电渗岩心夹持器、高温高压岩心夹持器、全直径岩心夹持器、金属填砂模型管、长岩心模型、非金属填砂模型管、径向流岩心夹持器、碳酸盐测定夹持器、孔隙度测定夹持器、动滤失岩心夹持器、双渗模型、达西定律模型、平面径向流模型、一维线性流模型、水电模拟实验装置、ZR中间容器、HC活塞耐酸容器、有机玻璃容器、高压观察窗容器、高温高压反应釜、视窗反应釜、压力调节器、回压阀、手动计量泵、手摇泵、电动计量泵、高压恒速泵、恒压恒速泵、双缸气体增压泵、采样器、加氢高压微反装置、小型固定流化床反应装置、催化反应设备、液固非均相催化反应装置、催化剂反应活性评价装置。
    高压水平阀、垂直阀、三通阀、四通阀、六通阀、单向阀、变丝接头、保护接头、死堵、接管压帽、卡环、仪表接头、高压快速接头、软管接头、取样器转样接头、内卡套过滤器、气瓶接头、手拧式快速接头、双卡套直通球阀、双卡套角式球阀、双卡套快开阀、软密封四通管接头、卡套式直通截止阀、卡套式直通节流止阀、卡套式角式截止阀、卡套式角式节流阀、卡套式角式截止阀、卡套式拧入管接头、卡套式焊接管接头、卡套式中间三通管接头、岩心夹持器专用皮套等。